By M. Ballauf, R.M. Crooks, B.I. III Lemon, M. Möller (Contributors)
ISBN-10: 354067828X
ISBN-13: 9783540678281
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Extra info for Topics in Current Chemistry 212, Dendrimers III Design, Dimersion, Function
Example text
21. This means that the time for flow-out of the powder becomes shorter with increasing functionality of the crosslinker, with respect to the total cycle time required for reaching satisfactory film properties (mechanical, chemical, Fig. 20, step D). The reduced flow-phase time results in a poorer film surface quality.
CERIUS2, Molecular Simulations, Waltham, MA, USA 47. Morgenroth F (1998) PhD thesis, University of Mainz 48. Dandliker PJ, Diederich F, Gisselbrecht J, Louati A, Gross M (1995) Angew Chem Int Ed Engl 34:2725; Angew Chem 107:2906 49. Kimura M, Shiba T, Muto T, Hanabusa K, Shirai H (1999) Macromolecules 32:8237 50. Newkome GR, Cardullo F, Constable EC, Moorefield CN, Thompson AMWC (1993) Chem Commun:925 51. Launay N, Caminade AM, Majoral JP (1995) J Am Chem Soc 117:3282 52. Wiesler U-M, Weil T, Dötz F, Müllen K (unpublished results) 53.
It was established in 1993 [12] that this reaction proceeds via an oxazolinium-carboxylate ion pair intermediate (Fig. 3). Ring opening of the oxazolinium species via nucleophilic attack of the associated carboxylate group affords the formation of the ester linkage. This picture is, however, incomplete because the dynamic nature of the amide bond is not taken into account. We have established through real-time IR spectroscopy that a rapid rearrangement of the hydroxyl-amide to the corresponding ester-amine (see Fig.
Topics in Current Chemistry 212, Dendrimers III Design, Dimersion, Function by M. Ballauf, R.M. Crooks, B.I. III Lemon, M. Möller (Contributors)
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