By A. Zecchina, E. Groppo, A. Damin (auth.), Christophe Copéret, Bruno Chaudret (eds.)
ISBN-10: 3540264965
ISBN-13: 9783540264965
Heterogeneous catalysis has been necessary to the advance of effective chemical tactics for greater than a century, and this box has been characteristically a part of the forged nation chemistry and floor technological know-how groups. The layout of higher catalysts has raised the next questions: "what is the constitution of the lively sites?" and "how to manage their nature?" the required have to improve extra sustainable chemical procedures and the luck of homogeneous catalysis hoping on molecular organometallic chemistry has led the group of molecular chemists to enquire the coaching of single-site heterogeneous catalysts. The authors speak about the molecular layout, the instruction, the characterisation and the catalytic purposes of well-defined oxides and steel debris. The readers will collect a molecular figuring out of heterogeneous catalysis, with a view to aid them boost a serious view and with a purpose to allure them to review this attention-grabbing field.
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Additional info for Surface and interfacial organometallic chemistry and catalysis
Sample text
Ferrari AM, Garrone E, Spoto G, Ugliengo P, Zecchina A (1995) Surf Sci 323:151 33. Weckhuysen BM, Schoonheydt RA, Jehng JM, Wachs IE, Cho SJ, Ryoo R, Kijlstra S, Poels E (1995) J Chem Soc Faraday Trans 91:3245 34. Weckhuysen BM, Verberckmoes AA, DeBaets AR, Schoonheydt RA (1997) J Catal 166:160 35. Vuurman MA, Wachs IE, Stufkens DJ, Oskam A (1993) J Mol Catal 80:209 36. Hardcastle FD, Wachs IE (1988) J Mol Catal 46:173 37. Dines TJ, Inglis S (2003) Phys Chem Chem Phys 5:1320 38. Thune PC, Linke R, van Gennip WJH, de Jong AM, Niemantsverdriet JW (2001) J Phys Chem B 105:3073 39.
5). 2 Oxidation Reactions Catalyzed by TS-1 The selective catalytic oxidation of organic compounds with an environmental attractive oxidant, aqueous H2 O2 , is a challenging goal of fine chemistry. Over the past two decades, heterogeneous Ti(IV)-based catalysts have received much attention for their application in this field. Highly active and selective catalysts can be produced by dispersing Ti atomically in a silica matrix [27, 28], or by grafting isolated Ti species to the surface of silica [29–31], mesoporous molecular sieves [32, 33], layered aluminosilicates [34], polyoxometallates [35, 36], or by isomorphously substituting Ti for silicon in molecular sieve frameworks [7, 17, 37–39].
38 2 Oxidation Reactions Catalyzed by TS-1 . . . . . . . . . . 8 Investigation of the Bare TS-1: Anhydrous Catalyst XRD . . . . . . . . . . . . . UV-Vis . . . . . . . . . . . . . XANES . . . . . . . . . . . . . EXAFS . . . . . . . . . . . . . IR . . . . . . . . . . . . . . Raman . . . . . . . . . . . . . Resonant Raman . . . . . . . . . . The Defective Nature of TS-1 Material: Speculative Model of Framework Sites .
Surface and interfacial organometallic chemistry and catalysis by A. Zecchina, E. Groppo, A. Damin (auth.), Christophe Copéret, Bruno Chaudret (eds.)
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